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Beilstein J. Org. Chem. 2015, 11, 1910–1916, doi:10.3762/bjoc.11.206
Graphical Abstract
Figure 1: Coordination motif of latent catalyst of olefin metathesis in which alkylidene ligand is bound to t...
Figure 2: Known latent catalysts of olefin metathesis in which alkylidene ligands are bound to a heteroatom, ...
Figure 3: Selected, known aryloxybenzylidene chelates [9,10].
Scheme 1: Synthesis of catalyst precursors 4–6 [11].
Scheme 2: Synthesis of catalysts 8–10.
Scheme 3: Synthesis of catalysts 13 and 14.
Figure 4: ROMP of COD. Conditions: CH2Cl2, 40 °C, 0.5 M, [COD]:[Ru] = 20000; For clarity, only two representa...
Figure 5: ROMP of cod. Conditions: CH2Cl2, 40 °C, 0.5 M, [cod]:[Ru] = 20000; For clarity only representative ...
Scheme 4: ROMP of monomer 15.
Figure 6: ROMP of monomer 15. Conditions: CDCl3, 40 °C, 0.08 M, [15]:[Ru] = 200.
Figure 7: ROMP of monomer 15. Conditions: CDCl3, 23 °C, 0.08 M, [15]:[Ru] = 200.
Scheme 5: Formation of phosphine free dimeric complex in the presence of CuCl.
Figure 8: A perspective view of complex 16, the ellipsoids are drawn at the 50% probability level. Hydrogen a...
Scheme 6: Synthesis of complexes 1a and 8 starting from dimer 16.
Scheme 7: Activation of complex 8 with one equivalent of HCl.